HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → N-(2-Aminoethyl)-2-(2,6-dichlorophenoxy)propanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | Ethyl 2-(2,6-dichlorophenoxy)propanoate | HCID 13177850 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-(2-Aminoethyl)-2-(2,6-dichlorophenoxy)propanamide | HCID 13177851 | 78.4% |
Reaction Steps
46.0 g (0.1748 mols) of (-)-2-(2,6-dichlorophenoxy)-propionic acid ethylester are stirred for 6 hours at room temperature with 212.0 g (3.527 mols) of 1,2-diaminoethane and, after working up, produce 38.0 g (-)-2-(2,6-dichlorophenoxy)-propionic acid-N-(2-aminoethyl)-amide, C11H14Cl2N2O2 [277.2] as a high viscosity oil, [α]D20 =-5.8° (c=1/ethanol)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04518783 |
| Source dataset | uspto-grants-1985_05 |
| ORD ID | ord-4e85bf5d297f41329ef4c9b741b894bb |
| Source note | uspto-grants-1985_05 |