ethyl P-methyl-2-nitro-5-chlorophenylphosphinate → ethyl P-methyl-2-nitro-5-(2-pyridyloxy)phenylphosphinate
Reaction equation
[CH3:1][P:2]([C:7]1[CH:12]=[C:11](Cl)[CH:10]=[CH:9][C:8]=1[N+:14]([O-:16])=[O:15])(=[O:6])[O:3][CH2:4][CH3:5].[N:17]1[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=1[OH:23]>>[CH3:1][P:2]([C:7]1[CH:12]=[C:11]([O:23][C:18]2[CH:19]=[CH:20][CH:21]=[CH:22][N:17]=2)[CH:10]=[CH:9][C:8]=1[N+:14]([O-:16])=[O:15])(=[O:6])[O:3][CH2:4][CH3:5]Participants
3
Procedure
Following the procedure of Example 17, ethyl P-methyl-2-nitro-5-chlorophenylphosphinate and 2-pyridyl alcohol are reacted together to give ethyl P-methyl-2-nitro-5-(2-pyridyloxy)phenylphosphinate.
Workup
- customare reacted together
Sources & evidence
- ORD record
- ord-f92e8ec9354e47bd9589719a6231269b
- Source dataset
- uspto-grants-1985_05
- Patent number
- US04520197
Reaction notes
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