HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 4-chloro-5-(2,4-dichlorophenoxy)benzo-2,1,3-oxadiazole N-oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 2-Chloro-3-(2,4-dichlorophenoxy)-6-nitroaniline | HCID 20264344 | — |
| Reactant | N-methylcarbonyl 2-chloro-3-(2,4-dichlorophenoxy)-6-nitroaniline | HCID 20264352 | — |
| Reactant | Sodium Hypochlorite | HCID 23665760 | — |
| Product | 4-chloro-5-(2,4-dichlorophenoxy)benzo-2,1,3-oxadiazole N-oxide | HCID 53750274 | — |
Reaction Steps
Following the procedure of Example 4, N-methylcarbonyl 2-chloro-3-(2,4-dichlorophenoxy)-6-nitroaniline is converted, by reaction with HCl, to 2-chloro-3-(2,4-dichlorophenoxy)-6-nitroaniline, which is then reacted with potassium hydroxide and sodium hypochlorite, again following Example 4 procedures, to yield the final product, 4-chloro-5-(2,4-dichlorophenoxy)benzo-2,1,3-oxadiazole N-oxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04544400 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-04bce43b8f9d420aa740cc9c2e7931dd |
| Source note | uspto-grants-1985_10 |