Pyridine → HCID 13575658, compound

Participants

Reaction Steps

To a solution of cyanuric fluoride (16 g, 0.12 mole in acetonitrile (125 ml) was added within 10 mins. a solution of oleic acid (80 g., 0.30 mole) and pyridine (24 g., 0.3 mole) in 125 ml. acetonitrile. The reaction mixture was stirred for 50 min and poured into ice-water, extracted with ether, and the organics dried over sodium sulfate. Removal of solvent and distillation in vacuo afforded oleoyl fluoride (85%, bp 184-186/12 torr).

Provenance & Evidence