HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trityl chloride → HCID 22825273, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trityl chloride | HCID 6456 | — |
| Reactant | (2S)-3-(Tetradecyloxy)propane-1,2-diol | HCID 12896846 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 22825273 | HCID 22825273 | — |
Reaction Steps
In 30 ml of dry pyridine, 2.82 g of 1-tetradecyl-sn-glycerol is allowed to react 3.27 g of triphenylchloromethane to give 1-tetradecyl-3-trityl-sn-glycerol. This compound is subjected to methylation with methyl iodide and deprotection to give 2 g of 1-tetradecyl-2-methyl-sn-glycerol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04544512 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-9fc64a9914ae4b66be1fbedac3538512 |
| Source note | uspto-grants-1985_10 |