HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → HCID 178476834, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 178476830 | HCID 178476830 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 178476834 | HCID 178476834 | 91.2% |
Reaction Steps
A solution of α-hydroxyethylphosphinic acid (5.5 g) and benzyl alcohol (2.26 g) in benzene (50 ml) was heated for 8 hours with removal of water through a Dean-Stark apparatus. After cooling, the reaction mixture was washed with water, dried over magnesium sulfate and concentrated in vacuo to give 3.65 g (91.2%) of benzyl α-hydroxyethylphosphinate (Compound No. 36).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04544652 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-3b10e5d9b7a94dba8dfc894d8aea4436 |
| Source note | uspto-grants-1985_10 |