Dimethylamine → HCID 20265071, compound

HRID 463760Notes

Reaction equation

HRID 463760 reaction equation
Br[CH2:2][C:3]1[CH:15]=[CH:14][C:6]2[O:7][C:8]([S:10](=[O:13])(=[O:12])[NH2:11])=[CH:9][C:5]=2[CH:4]=1.[CH3:16][NH:17][CH3:18]>CO>[CH3:16][N:17]([CH2:2][C:3]1[CH:15]=[CH:14][C:6]2[O:7][C:8]([S:10](=[O:13])(=[O:12])[NH2:11])=[CH:9][C:5]=2[CH:4]=1)[CH3:18]

Participants

4

Reactant 2

HCID 674DimethylamineHCID 20265088HCID 20265088, compound

Product 1

HCID 20265071HCID 20265071, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

An ice cold, stirred solution of 5-bromomethyl-2-sulfamoylbenzo[b]furan in methanol is treated with an excess of anhydrous dimethylamine to give the title compound.

Sources & evidence

ORD record
ord-23a8764a1231440aa2ff40bd2d716081
Source dataset
uspto-grants-1985_10
Patent number
US04544667

Reaction notes

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