HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl sulfate(1-) → 3,5-Dimethyl-1,3,5-oxadiazinane-2,4,6-trione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl sulfate(1-) | HCID 4694097 | — |
| Reactant | 3-Methyl-1,3,5-oxadiazinane-2,4,6-trione | HCID 20265335 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | 3,5-Dimethyl-1,3,5-oxadiazinane-2,4,6-trione | HCID 12455323 | 92% |
Reaction Steps
The process disclosed in example 1 is used, except that the solvent is not distilled. 15.1 g of methyl sulfate (0.12 mole) are added to the solution of 3-methyl-1,3,5-oxadiazine-2,4,6-trione. The solvent is evaporated after 10 minutes of reaction at a temperature of 25° C. After washing with water and carbon tetrachloride, 14.6 g of 3,5-dimethyl-1,3,5-oxadiazine-2,4,6-trione (yield: 92%) which is a symmetrical disubstituted 1,3,5-oxadiazine trione are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04544743 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-b4e8bd624fac475eb35b2251357ce230 |
| Source note | uspto-grants-1985_10 |