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O-Allylhydroxylamine hydrochloride → 2-Allyloxyimino-2-(3-chloro-4-hydroxyphenyl)acetic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | O-Allylhydroxylamine hydrochloride | HCID 3084724 | — |
| 反応物 | 2-(3-Chloro-4-hydroxyphenyl)-2-oxoacetic acid | HCID 12961139 | — |
| 生成物 | 2-Allyloxyimino-2-(3-chloro-4-hydroxyphenyl)acetic acid | HCID 136210784 | 98.1% |
反応手順
2-(3-Chloro-4-hydroxyphenyl)glyoxylic acid (2 g.) and O-allylhydroxylamine hydrochloride (1.1 g.) were reacted according to a similar manner to that of Preparation 5-2)(a) to give oil of 2-allyloxyimino-2-(3-chloro-4-hydroxyphenyl)acetic acid (syn isomer) (2.5 g.).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04544653 |
| 出典データセット | uspto-grants-1985_10 |
| ORD ID | ord-f8d85d1db7b1412fadc04662059775e1 |
| 出典メモ | uspto-grants-1985_10 |