HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → Methyl 4-chlorobenzene-1-carboximidothioate hydroiodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 4-Chlorothiobenzamide | HCID 2734826 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | Methyl 4-chlorobenzene-1-carboximidothioate hydroiodide | HCID 2777317 | — |
Reaction Steps
A 17.16 g portion of 4-chlorothiobenzamide was dissolved in 80 ml of acetone and 15.14 g of methyl iodide was added. The mixture was stirred for 2 hours and then the solid was collected, washed with acetone and dried, giving 21.3 g of 4-chlorobenzenecarboximidothioic acid, methyl ester, hydroiodide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04544759 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-1ede6d8960aa44a1ae0763510bf475ee |
| Source note | uspto-grants-1985_10 |