HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isoamyl Nitrite → Ethyl 2-hydroxyimino-2-(1,2,5-thiadiazol-3-yl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isoamyl Nitrite | HCID 8053 | — |
| Reactant | Ethyl 2-(1,2,5-thiadiazol-3-yl)acetate | HCID 12906551 | — |
| Product | Ethyl 2-hydroxyimino-2-(1,2,5-thiadiazol-3-yl)acetate | HCID 136180295 | — |
Reaction Steps
Ethyl 2-(1,2,5-thiadiazol-3-yl)acetate (9.5 g.) and isopentyl nitrite (10 ml.) were reacted according to a similar manner to that of Example 3(a)(1) to give ethyl 2-hydroxyimino-2-(1,2,5-thiadiazol-3-yl)acetate (a mixture of syn and anti isomers) (10.5 g.), mp 60° to 66° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04544751 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-74846a22f5d843c4b3149f854d228170 |
| Source note | uspto-grants-1985_10 |