HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloroacetyl chloride → 2-Dichloroacetoxyimino-2-(1,2,5-thiadiazol-3-yl)acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloroacetyl chloride | HCID 6593 | — |
| Reactant | 2-Hydroxyimino-2-(1,2,5-thiadiazol-3-yl)acetic acid | HCID 136138613 | — |
| Product | 2-Dichloroacetoxyimino-2-(1,2,5-thiadiazol-3-yl)acetic acid | HCID 54347826 | 47% |
Reaction Steps
2-Hydroxyimino-2-(1,2,5-thiadiazol-3-yl)acetic acid (syn isomer) (4.8 g.) and dichloroacetyl chloride (9.2 g.) were reacted according to a similar manner to that of Example 6(a)(4) to give crystals of 2-dichloroacetoxyimino-2-(1,2,5-thiadiazol-3-yl)acetic acid (syn isomer) (3.7 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04544751 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-56b880791e6542d8958bba7dbddc1830 |
| Source note | uspto-grants-1985_10 |