HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 12624437, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Ethyl nitroacetate | HCID 69379 | — |
| Reactant | 2-Hydrazinylidene-1,2-diphenylethanone | HCID 79289 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 12624437 | HCID 12624437 | — |
Reaction Steps
8.96 g (0.040 mole) of benzilmonohydrazone, 5.3 g (0.040 mole) of ethylnitroacetate and 4.8 g (0.056 mole) of piperidine in 100 mL of benzene were heated in a round bottom flask with a Dean-Stark trap and condenser for 24 hrs.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04545810 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-c29953d81a0647d0821e6b7c1b1b2710 |
| Source note | uspto-grants-1985_10 |