HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18599480, compound → HCID 18599483, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18599480 | HCID 18599480 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 18599483 | HCID 18599483 | 36.7% |
Reaction Steps
Hydrolysis of fraction 2 (2% acetone), as above, gave: 3α-hydroxy-7-methyl-5β-chol-6-enoic acid (3.0 g, mp, 121°-122° C.). Hydrolysis of fraction 3, (2% acetone), as above, gave 3α-hydroxy-7-methylene-5β-cholanoic acid (1.1 g.; m.p. 104°-105° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04545938 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-530f89b4afcb4cdabc8ccdaf44e31219 |
| Source note | uspto-grants-1985_10 |