HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 9868175, compound → 3-Hydroxy-7-methylcholan-24-oic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 9868175 | HCID 9868175 | — |
| Reactant | HCID 18599479 | HCID 18599479 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 3-Hydroxy-7-methylcholan-24-oic acid | HCID 126016 | — |
Reaction Steps
The compounds obtained from fractions 2 and 3 from Example 2, above, were dissolved in ethyl acetate and reduced with hydrogen in the presence of a PtO2 catalyst to yield a mixture of 3α-hydroxy-7α-methyl-5β-cholanic acid and 3α-hydroxy-7β-methyl-5β-cholanic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04545938 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-f1c7d0bbb8324c94ba24235899d7405b |
| Source note | uspto-grants-1985_10 |