Carbon Disulfide → HCID 20263992, compound

HRID 464064Notes

Reaction equation

HRID 464064 reaction equation
Cl.[CH:2]([C:4]1[C:9]([OH:10])=[C:8]([CH2:11]O)[C:7]([CH2:13][OH:14])=[CH:6][N:5]=1)=[CH2:3].[OH-].[Na+].C(=S)=[S:18]>>[CH:2]([C:4]1[C:9]([OH:10])=[C:8]([CH2:11][SH:18])[C:7]([CH2:13][OH:14])=[CH:6][N:5]=1)=[CH2:3]

Participants

4

Reactant 3

HCID 6348Carbon DisulfideHCID 14798Sodium HydroxideHCID 70492662HCID 70492662, compound

Product 1

HCID 20263992HCID 20263992, compound

Procedure

The product from Step F is treated with sodium hydroxide and carbon disulfide as described in Example 1, Step C, to produce 2-vinyl-3-hydroxy-4-mercaptomethyl-5-hydroxymethylpyridine.

Sources & evidence

ORD record
ord-e2dbfd989c2a40e3a469b689dee815ba
Source dataset
uspto-grants-1985_10
Patent number
US04546106

Reaction notes

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