HuagongsheHuagongshe Chemistry Print Report · For research reference only
[6-(Hydroxymethyl)pyridin-3-yl]methanol → 5-(Hydroxymethyl)pyridine-2-carboxaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | [6-(Hydroxymethyl)pyridin-3-yl]methanol | HCID 820251 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 5-(Hydroxymethyl)pyridine-2-carboxaldehyde | HCID 13518562 | — |
Reaction Steps
2,5-Di(hydroxymethyl)pyridine (10 g.) in 300 ml. of hot chloroform is treated with 100 g of manganese dioxide. After 1/2 hour of stirring, the mixture is filtered and the filtrate is evaporated to dryness to give 2-formyl-5-hydroxymethylpyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04546106 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-bd310b86aab94d3a98f09655062f091e |
| Source note | uspto-grants-1985_10 |