HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Iodoaniline → HCID 14099777, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Iodoaniline | HCID 10893 | — |
| Reactant | Benzonitrile, 4-(iodoacetyl)- | HCID 143737 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14099777 | HCID 14099777 | — |
Reaction Steps
p-Cyanophenacyl iodide (18.0 g, 0.08 mole) was combined with p-iodoaniline (35.2 g, 0.16 mole) in 32.1 g of absolute ethanol and stirred 16 hours. Precipitated title product was recovered by filtration and repulped in 400 ml ether: 42.4 g; m.p. 160°-165°; ms 362, 232, 219.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04546113 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-e3576956eda742c7bcb17e5111e94ccf |
| Source note | uspto-grants-1985_10 |