HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allylamine → 925-02-0
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allylamine | HCID 7853 | — |
| Reactant | Maleic Anhydride | HCID 7923 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 925-02-0 | HCID 1551409 | — |
Reaction Steps
Allylamine reacts readily with maleic anhydride in THF to give N-allylmaleamic acid (VIII) in quantitative yield. VIII reacts with bisulfite in water to form 3-carboxy-3-sulfo-N-allyl propionamide (IX). At 160° C., (IX) cyclolyzes slowly to form N-allyl-sulfo-succinimide (X).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04546156 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-0b8ea43df03d4343a915c78881d8d953 |
| Source note | uspto-grants-1985_10 |