HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → Azobisisobutyronitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-Amino-2-methylpropionitrile | HCID 88022 | — |
| Reactant | Sodium Bromide | HCID 253881 | — |
| Product | Azobisisobutyronitrile | HCID 6547 | — |
Reaction Steps
By method of Example 2, 2-amino-2-methylpropanenitrile (of 78.5% purity) was dichlorinated and coupled with further 2-amino-2-methylpropanenitrile in the presence of caustic soda and the following combinations of tetra alkyl quaternary ammonium chloride surfactant and added sodium bromide. The yields of title compound obtained were as shown.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04546174 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-178ee1dfd303447ca4ba4424949f1b22 |
| Source note | uspto-grants-1985_10 |