Cyclohexane, (bromomethyl)- → HCID 20262924, compound

HRID 464314Notes

Reaction equation

HRID 464314 reaction equation
[ClH:1].[CH2:2]1[C:7]2[C:8](=[O:16])[C:9]3[CH:15]=[CH:14][CH:13]=[CH:12][C:10]=3[S:11][C:6]=2[CH2:5][CH2:4][NH:3]1.Br[CH2:18][CH:19]1[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]1>>[ClH:1].[CH:19]1([CH2:18][N:3]2[CH2:4][CH2:5][C:6]3[S:11][C:10]4[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=4[C:8](=[O:16])[C:7]=3[CH2:2]2)[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]1

Participants

3

Reactant 2

HCID 137636Cyclohexane, (bromomethyl)-HCID 20262908HCID 20262908, compound

Product 1

HCID 20262924HCID 20262924, compound

Procedure

Using the procedure of Example 19, 1,2,3,4-tetrahydro-10H-(1)-benzothiopyrano[3,2-c]pyridin-10-one hydrochloride and bromomethylcyclohexane were reacted to obtain 2-cyclohexylmethyl-1,2,3,4-tetrahydro-10H-(1)-benzothiopyrano[3,2-c]pyridin-10-one hydrochloride with the melting point and analysis of Table II.

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-69c10dd1366b42a3b208c02b49a0ddc5
Source dataset
uspto-grants-1985_10
Patent number
US04547507

Reaction notes

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