HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophenol → N-benzyloxycarbonyl-glycine-phenythio ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | Benzyloxycarbonylglycine | HCID 14349 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-benzyloxycarbonyl-glycine-phenythio ester | HCID 22764889 | 62% |
Reaction Steps
Using thiophenol and Z-Gly.OH, Example 78 was repeated; except that dichloromethane was used in place of ethyl acetate as the extraction solvent, to obtain N-benzyloxycarbonyl-glycine-phenythio ester (hereinafter represented by ##STR12## in a yield of 62%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04173563 |
| Source dataset | uspto-grants-1979_11 |
| ORD ID | ord-01bd8ea14e7b4957854705e522f04f34 |
| Source note | uspto-grants-1979_11 |