Sodium Dithionite → HCID 54164473, compound

HRID 464607Notes

Reaction equation

HRID 464607 reaction equation
[NH2:1][C:2]1[N:7]([CH2:8][C:9]([CH3:12])([CH3:11])[CH3:10])[C:6](=[O:13])[NH:5][C:4](=[O:14])[C:3]=1[N:15]=O.S(S([O-])=O)([O-])=O.[Na+].[Na+]>O>[NH2:15][C:3]1[C:4](=[O:14])[NH:5][C:6](=[O:13])[N:7]([CH2:8][C:9]([CH3:10])([CH3:11])[CH3:12])[C:2]=1[NH2:1]

Participants

4

Reactant 2

HCID 24489Sodium DithioniteHCID 53832834HCID 53832834, compound

Product 1

HCID 54164473HCID 54164473, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

To a suspension of 6.0 g of XXVII in 100 ml of water was added 13.0 g of sodiumdithionite in portions. The green crystals were filtered off and washed with water. Yield 4.0 g (XXVIII).

Workup

  1. filtrationThe green crystals were filtered off
  2. washwashed with water

Sources & evidence

ORD record
ord-caec3b0a04b24c4487518c44da5e6192
Source dataset
uspto-grants-1985_10
Patent number
US04548818

Reaction notes

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