HCID 13457229, compound → HCID 70042494, compound

HRID 464636Notes

Reaction equation

HRID 464636 reaction equation
[Cl:1][C:2]1[C:7]([Cl:8])=[CH:6][CH:5]=[CH:4][C:3]=1[CH:9]1[C:14]([C:15]([O:17][CH3:18])=[O:16])=[C:13]([CH3:19])[NH:12][C:11]([CH2:20][O:21][CH2:22][C:23]([NH2:25])=[S:24])=[C:10]1[C:26]([O:28][CH2:29][CH3:30])=[O:27].O.Cl>>[NH2:12][CH2:11][CH2:10][C:9]1[N:25]=[C:23]([CH2:22][O:21][CH2:20][C:11]2[NH:12][C:13]([CH3:19])=[C:14]([C:15]([O:17][CH3:18])=[O:16])[CH:9]([C:3]3[CH:4]=[CH:5][CH:6]=[C:7]([Cl:8])[C:2]=3[Cl:1])[C:10]=2[C:26]([O:28][CH2:29][CH3:30])=[O:27])[S:24][CH:3]=1

Participants

3

Reactant 2

HCID 13457229HCID 13457229, compoundHCID 21885828Hydrate;hydrochloride

Product 1

HCID 70042494HCID 70042494, compound

Procedure

This compound was prepared by the method described in Example 41 but using 2-{[4-(2,3-dichlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyridin-2-yl]methoxy}thioacetamide as starting material. The product was characterised as a hydrochloride monohydrate, m.p. 110°-112° C. Found: C,48.44; H,4.99; N,7.15. C24H27Cl2N3O5S.HCl.H2O requires: C,48.44; H,5.04; N,7.06%.

Workup

  1. customThis compound was prepared by the method

Sources & evidence

ORD record
ord-561b94f7f9aa40119ed601ad0bb4060d
Source dataset
uspto-grants-1985_10
Patent number
US04548935

Reaction notes

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