HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 54424797, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | 2,3-Dihydro-1H-inden-1-one oxime | HCID 302323 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 54424797 | HCID 54424797 | — |
Reaction Steps
A solution of p-toluenesulfonyl chloride (266 g) in pyridine (300 ml) was added dropwise to a stirred solution of 2,3-dihydro-1-hydroxyimino-1H-indene (100.8 g) in pyridine (600 ml) at 0°-5°. The mixture was stirred for 3 hours at 0°, then was poured into water and the title compound filtered. This was washed several times with water and air-dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04548943 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-f5967bb067124555a90763e6955cea3a |
| Source note | uspto-grants-1985_10 |