反应详情

A suspension of 300 g of 3,4-dichlorocinnamic acid (J. Org. Chem., 26:2991 (1961)) and 25 ml of concentrated sulfuric acid in 1.7 liters of methanol is heated to reflux for 24 hours. The solution is concentrated, cooled, and filtered to give as a white solid, 3,4-dichlorocinnamic acid methyl ester, mp 114°-15° C.

1. temperatureis heated
2. temperatureto reflux for 24 hours
3. concentrationThe solution is concentrated
4. temperaturecooled
5. filtrationfiltered