反应详情

A suspension of 300 g of 4-methoxycinnamic acid (J. Chem. Soc., Chem. Comm., 355, (1978)) and 25 ml of concentrated sulfuric acid in 1.7 liters of methanol is heated to reflux for 96 hours. The solution is concentrated, cooled, and filtered to give as a white solid, 4-methoxycinnamic acid methyl ester, mp 85°-86° C.

1. temperatureis heated
2. temperatureto reflux for 96 hours
3. concentrationThe solution is concentrated
4. temperaturecooled
5. filtrationfiltered