HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-2-phenylpent-4-enal → 2-Methyl-2-phenylpent-4-en-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-2-phenylpent-4-enal | HCID 91177 | — |
| Reactant | HCID 20262662 | HCID 20262662 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-Methyl-2-phenylpent-4-en-1-ol | HCID 3019061 | 96% |
Reaction Steps
Following the procedure of part (a) of Example I a 400 g sample of 2-methyl-2-phenyl-4-pentenal was reduced with 30 g of lithium aluminum hydride in 1200 ml of anhydrous ether. Usual workup and distillation afforded 386 g (96% yield) of the desired 2-methyl-2-phenyl-4-penten-1-ol (bp 112°-114° C./0.5 mm Hg) with a purity of 97%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04549029 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-4955e48d50034fce96cd5a9c8683bc0e |
| Source note | uspto-grants-1985_10 |