HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 464805Generated: October 30, 2026
Piperidine → Piperidine, 1-(2-phenoxyethyl)-
https://huagongshe.com/reaction/464805
Participants
| Role | Name | HCID | Charge |
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| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Benzene, (2-bromoethoxy)- | HCID 68526 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Piperidine, 1-(2-phenoxyethyl)- | HCID 120169 | 96.4% |
Reaction Steps
A mixture of 20 g of 2-phenoxyethyl bromide thus obtained, 7.92 g of piperidine and 12.86 g of potassium carbonate was added into 100 ml of ethyl alcohol and stirred for 6 hours at 100° C. The mixture obtained was filtered and condensed under reduced pressure to give 18.4 g of 1-(2-phenoxyethyl)piperidine having a boiling point of 111° C. to 112° C. at 7 mmHg in a yield of 90%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04549023 |
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| Source dataset | uspto-grants-1985_10 |
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| ORD ID | ord-cf3aca30e2494015a09b14543274abe8 |
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| Source note | uspto-grants-1985_10 |
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