Sodium Carbonate → 2-(5-Methyl-4-imidazolylmethylthio)ethyl N-methyl-dithiocarbamate dithiocarbamate

HRID 46482Notes

Reaction equation

HRID 46482 reaction equation
Cl.[CH3:2][C:3]1[NH:7][CH:6]=[N:5][C:4]=1[CH2:8][S:9][CH2:10][CH2:11][S:12][C:13](=[S:16])[NH:14][CH3:15].C(=O)([O-])[O-].[Na+].[Na+]>>[C:13](=[S:12])([SH:16])[NH2:14].[CH3:15][NH:14][C:13](=[S:16])[S:12][CH2:11][CH2:10][S:9][CH2:8][C:4]1[N:5]=[CH:6][NH:7][C:3]=1[CH3:2]

Participants

3

Reactant 2

HCID 10340Sodium CarbonateHCID 887953812-(5-methyl-4-imidazolylmethylthio)ethyl-N-methyldithiocarbamate hydrochloride

Product 1

HCID 887956432-(5-Methyl-4-imidazolylmethylthio)ethyl N-methyl-dithiocarbamate dithiocarbamate

Procedure

This hydrochloride may be treated with aqueous sodium carbonate and the mixture extracted with chloroform and the chloroform extracts evaporated to give the free base.

Workup

  1. extractionthe mixture extracted with chloroform
  2. customthe chloroform extracts evaporated
  3. customto give the free base

Sources & evidence

ORD record
ord-239f1410b5ca4f5e9ded91dd5d3b6cab
Source dataset
uspto-grants-1979_11
Patent number
US04173644

Reaction notes

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