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HRID464912

反应详情

EQUATION

反应方程式

HRID 464912 的结构方程式

REACTANTS

反应物

2
结构：CC(Oc1ccc(Oc2ccc(C(F)(F)F)cc2)cc1)C(=O)O
HCID181206

Trifop

C16H13F3O4

结构：O=C=NS(=O)(=O)c1cc(Cl)ccc1Cl
HCID12875187

2,5-Dichlorobenzene-1-sulfonyl isocyanate

C7H3Cl2NO3S

PRODUCTS

生成物

1
结构：CC(Oc1ccc(Oc2ccc(C(F)(F)F)cc2)cc1)C(=O)NS(=O)(=O)c1cc(Cl)ccc1Cl
HCID13505617

未命名化合物

PROCEDURE

实验过程

A solution of one gram (0.0031 mole) 2-[4-(4-trifluoromethylphenoxy)phenoxy]-propionic acid in dry CHCH3 was treated with 0.8 gram (g) (0.0081 mole) 2,5-dichlorobenzene sulfonyl isocyanate. The solution was stirred for approximately 18 hours, then heated to reflux for three hours, followed by cooling.

WORKUP

后处理

  1. temperatureheated
  2. temperatureto reflux for three hours
  3. temperatureby cooling