HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic acid, 2-(4-nitrophenyl)hydrazide → Acetic acid, 2-(4-aminophenyl)hydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic acid, 2-(4-nitrophenyl)hydrazide | HCID 3404344 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Acetic acid, 2-(4-aminophenyl)hydrazide | HCID 81068 | 75% |
Reaction Steps
16.6 g of 1-acetyl-2-(4-nitrophenyl)hydrazine was catalytically reduced at room temperature in 800 ml of ethanol using a palladium-carbon catalyst. The reaction solution was filtered and cooled to obtain 10.5 g of 1-acetyl-2-(4-aminophenyl)hydrazine. Yield: 75%. Melting point: 130°-140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04550070 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-7a3fe1e4449845768c28bfa4bc3276d2 |
| Source note | uspto-grants-1985_10 |