HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dihydro-2,4-dimethyl-7-nitrobenzofuran → HCID 13575669, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dihydro-2,4-dimethyl-7-nitrobenzofuran | HCID 13575668 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 13575669 | HCID 13575669 | — |
Reaction Steps
A mixture of 24.3 g of 1C, 200 ml of tetrahydrofuran (THF) and 2 g of activated Raney nickel catalyst was treated with hydrogen (40 psig) in a Parr shaker three hours, then filtered. The solvent was evaporated from the filtrate to give 7-amino-2,3-dihydro-2,4-dimethylbenzofuran (1D), as an amber syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04550121 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-d11b2d305be64229a697beedc72a21a3 |
| Source note | uspto-grants-1985_10 |