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Dimethyl-(2-piperidin-2-yl-ethyl)-amine → 5,10-Dihydro-5-[[2-[2-(dimethylamino)ethyl]-1-piperidinyl]-acetyl]-11H-dibenzo[b,e][1,4]diazepin-11-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethyl-(2-piperidin-2-yl-ethyl)-amine | HCID 296295 | — |
| 反応物 | 5-(chloroacetyl)-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one | HCID 10085419 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | 5,10-Dihydro-5-[[2-[2-(dimethylamino)ethyl]-1-piperidinyl]-acetyl]-11H-dibenzo[b,e][1,4]diazepin-11-one | HCID 13578559 | — |
反応手順
The title compound is prepared analogously to Example 2 from 5-(chloroacetyl)-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one and 2-[2-(dimethylamino)ethyl]piperidine to give colorless crystals, mp. 155°-157° C. (acetonitrile).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04550107 |
| 出典データセット | uspto-grants-1985_10 |
| ORD ID | ord-60e390bd0a8b45b6a7d430164a616997 |
| 出典メモ | uspto-grants-1985_10 |