HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 20261919, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | (+-)-Tetramisole | HCID 3913 | — |
| Reactant | Bromoacetic Acid | HCID 6227 | — |
| Product | HCID 20261919 | HCID 20261919 | 81% |
Reaction Steps
2 g (0.01 mol) of 2,3,5,6-tetrahydro-6-phenylimidazo-[2,1-b]-thiazole are dissolved in 20 ml of acetone and added with 1.53 g (0.01 mol) of methyl ester of monobromacetic acid. After 12 hours the residue is filtered-off and washed with acetone to give 2.86 g (81%) of 2,3,5,6-tetrahydro-6-phenyl-7-methoxycarbonylmethylimidazo-[2,1-b]-thiazolium bromide melting at 81°-82° C. (from dioxane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04550170 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-282bffce6faf4ef09327d9ede0c4e36e |
| Source note | uspto-grants-1985_10 |