HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl orthoacetate → HCID 13533707, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl orthoacetate | HCID 66221 | — |
| Reactant | 2'-Hydrazino-2,4'-bipyridine | HCID 13533717 | — |
| Product | HCID 13533707 | HCID 13533707 | — |
Reaction Steps
A mixture of 2.0 g of 2'-hydrazino-2,4'-bipyridine and 50 ml of triethyl orthoacetate was heated on a steam bath for 18 hours, then chilled, filtered and the crystals washed with hexane. These crystals were recrystallized from methylene chloride, giving 1.8 g of the desired product as white crystals, mp 239°-241° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04550166 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-9108f3fd2f154bc78e71c702367ba9e6 |
| Source note | uspto-grants-1985_10 |