HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl orthoformate → HCID 13533712, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl orthoformate | HCID 31214 | — |
| Reactant | HCID 13533720 | HCID 13533720 | — |
| Product | HCID 13533712 | HCID 13533712 | — |
Reaction Steps
A mixture of 1.7 g of 2'-hydrazino-2,3'-bipyridine and 50 ml of triethyl orthoformate was heated on a steam bath for 3 hours. Standing and chilling gave crystals which were collected, washed with hexane and dried, giving 1.5 g of the desired product as cream colored crystals, mp 212°-214° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04550166 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-c419a8dacb314dceb06e1b1a9ac105cc |
| Source note | uspto-grants-1985_10 |