HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86740397, compound → HCID 86740414, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86740397 | HCID 86740397 | — |
| Reactant | HCID 86740415 | HCID 86740415 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86740414 | HCID 86740414 | 24.6% |
Reaction Steps
To a solution of 0.250 g of sodium (3R,4R)-3-[2-(2-chloroacetamidothiazol-4-yl)-2-methoxyiminoacetamido]-4-methylthio-2-oxoazetidine-1-sulfonate in 8 ml of water is added under ice-cooling 0.078 g of sodium monomethyldithiocarbamate, and the mixture is stirred at room temperature for 1.5 hours. The same procedure as Example 3B yields 0.052 g of sodium (3R,4R)-3-[2-(2-aminothiazol-4-yl)-2-methoxyiminoacetamido]-4-methylthio-2-oxoazetidine-1-sulfonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04550105 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-dfc7d32d35ab46fcbf01e6dc7d7f64d6 |
| Source note | uspto-grants-1985_10 |