HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(3-benzoylthiopropanoyl)-L-alanine → N-(3-Sulfanylpropanoyl)-L-leucine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(3-benzoylthiopropanoyl)-L-alanine | HCID 13036931 | — |
| Reactant | N-[3-(Benzoylsulfanyl)propanoyl]-L-leucine | HCID 13036933 | — |
| Product | N-(3-Sulfanylpropanoyl)-L-leucine | HCID 13036942 | — |
Reaction Steps
By substituting N-(3-benzoylthiopropanoyl)-L-leucine (6.46 g.) for the N-(3-benzoylthiopropanoyl)-L-alanine in the procedure of Example 2, 2.75 g. of N-(3-mercaptopropanoyl)-L-leucine are obtained, m.p. 131°-132°. This material is recrystallized from acetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04173704 |
| Source dataset | uspto-grants-1979_11 |
| ORD ID | ord-277d954700524ba6b2a5e462eb3e64a2 |
| Source note | uspto-grants-1979_11 |