HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67895971, compound → HCID 19874535, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67895971 | HCID 67895971 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19874535 | HCID 19874535 | 86.7% |
Reaction Steps
1-Benzyl-4-[4-(2,2-ethylenedioxypropyl)phenyl]piperidin-4-ol (10.7 g) in methanol, was hydrogenated at room temperature and pressure over 10% palladium on carbon (5.0 g). After filtration through celite and evaporation of the solvent in vacuo, the residue was crystallised from ethanol:ether to give 4-[4-(2,2-ethylenedioxypropyl)phenyl]piperidin-4-ol (7.0 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05153210 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-38eb3b646560413190c13b2d1d7df824 |
| Source note | uspto-grants-1992_10 |