HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 2-Methoxybenzoylacetonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | Bromomethyl 2-methoxyphenyl ketone | HCID 123440 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-Methoxybenzoylacetonitrile | HCID 4962750 | — |
Reaction Steps
A 10.0 g. portion of α-bromo-o-methoxyacetophenone is suspended in 50 ml. of ethanol. A solution of 6.4 g. of sodium cyanide in 30 ml. of water is added as described in Example 38. Following the procedure of Example 38, there is obtained o-methoxybenzoylacetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04173650 |
| Source dataset | uspto-grants-1979_11 |
| ORD ID | ord-c92257dc890c478997046b240e38ba71 |
| Source note | uspto-grants-1979_11 |