HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54258336, compound → HCID 10317467, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54258336 | HCID 54258336 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 10317467 | HCID 10317467 | — |
Reaction Steps
A solution of 1.385 g of ethyl 3-[3-(3-pyridyl)propyl]-7-(2-tetrahydropyranyloxy)-hept-2-enoate in 30 ml ethyl acetate is hydrogenated in a Parr apparatus at 3 atmospheres (=3.04 bar) pressure and room temperature in the presence of 5% Pd/C catalyst for 13 h to yield ethyl 3-[3-(3-pyridyl)propyl]-7-(2-tetrahydropyranyloxy)-heptanoate; NMR (CDCl3): delta 2.2 (ddd,2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05153214 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-c946449696d24b17867f1c9e3bebe3b3 |
| Source note | uspto-grants-1992_10 |