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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 465611Generated: October 29, 2026

4-Chlorobenzenesulfonyl chloride → HCID 14986711, compound

https://huagongshe.com/reaction/465611

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Chlorobenzenesulfonyl chlorideHCID 7398—
ReactantHCID 14986710HCID 14986710—
ProductHCID 14986711HCID 14986711—

Reaction Steps

Ethyl 8-amino-5-(3-pyridyloxy)-octanoate is condensed with p-chlorophenylsulfonyl chloride according to methodology previously described to yield ethyl 8-(p-chlorophenylsulfonamido)-5-(3-pyridyloxy)-octanoate which is purified by chromatography on silica gel using 7:3 ethyl acetate/hexane as eluent; 1H-NMR (CDCl3): delta 8.26 (br,1H), 8.20 (br,4H), 5.23 (t,1H), 4.28 (m,1H), 4.08 (q,2H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05153214
Source datasetuspto-grants-1992_10
ORD IDord-4a445bbb422a468f87d6c977134196f9
Source noteuspto-grants-1992_10