Phenyl isocyanate → HCID 53876747, compound

HRID 465650Notes

Reaction equation

HRID 465650 reaction equation
[NH2:1][C@@H:2]([CH2:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)[C:3]([NH:5][C:6]1[C:11]([F:12])=[CH:10][C:9]([F:13])=[CH:8][C:7]=1[F:14])=[O:4].[C:22]1([N:28]=[C:29]=[O:30])[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1>>[C:22]1([NH:28][C:29]([NH:1][C@@H:2]([CH2:15][C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)[C:3]([NH:5][C:6]2[C:7]([F:14])=[CH:8][C:9]([F:13])=[CH:10][C:11]=2[F:12])=[O:4])=[O:30])[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1

Participants

3

Reactant 2

HCID 7672Phenyl isocyanateHCID 53938717HCID 53938717, compound

Product 1

HCID 53876747HCID 53876747, compound

Procedure

Following the procedure of Example 58 only using the product of Example 50 and phenylisocyanate, the title compound was obtained, mp 225°-233° C.

Sources & evidence

ORD record
ord-d3308a0ae4dd44c888aa430a088aef71
Source dataset
uspto-grants-1992_10
Patent number
US05153226

Reaction notes

Loading…