HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isothiocyanic acid, p-dimethylaminophenyl ester → N-[2,6-bis(1-Methylethyl)phenyl]-2-[[[[4-(dimethylamino)phenyl]amino]thioxomethyl](phenylmethyl)amino]acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isothiocyanic acid, p-dimethylaminophenyl ester | HCID 75047 | — |
| Reactant | N-[2,6-bis(1-Methylethyl)phenyl]-2-[(2,2-diphenylethyl)amino]acetamide | HCID 19874997 | — |
| Product | N-[2,6-bis(1-Methylethyl)phenyl]-2-[[[[4-(dimethylamino)phenyl]amino]thioxomethyl](phenylmethyl)amino]acetamide | HCID 19874983 | — |
Reaction Steps
When in the procedure of Example 80 an appropriate amount of the product of Example 71 was substituted for the product of Example 70 and an appropriate amount of 4-dimethylaminophenylisothiocyanate was substituted for ethyl isocyanato acetate the title compound was obtained. Total yield, 0.84 g (80%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05153226 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-85e7b112d9134592a890337d9c27b1c6 |
| Source note | uspto-grants-1992_10 |