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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 465659Generated: October 25, 2026

Isothiocyanic acid, p-dimethylaminophenyl ester → N-[2,6-bis(1-Methylethyl)phenyl]-2-[[[[4-(dimethylamino)phenyl]amino]thioxomethy](diphenylmethyl)amino]acetamide

https://huagongshe.com/reaction/465659

Reaction equation

Participants

RoleNameHCIDCharge
ReactantIsothiocyanic acid, p-dimethylaminophenyl esterHCID 75047—
ReactantN-[2,6-bis(1-Methylethyl)phenyl]-2-[(diphenylmethyl)amino]acetamideHCID 1645639—
ReactantN-[2,6-bis(1-Methylethyl)phenyl]-2-[(2,2-diphenylethyl)amino]acetamideHCID 19874997—
ProductN-[2,6-bis(1-Methylethyl)phenyl]-2-[[[[4-(dimethylamino)phenyl]amino]thioxomethy](diphenylmethyl)amino]acetamideHCID 86746182—

Reaction Steps

When in the procedure of Example 80 an appropriate amount of 4-dimethylaminophenylisothiocyanate was substituted for ethyl isocyanato acetate and an appropriate amount of the product of Example 4 was substituted for the product of Example 70 and the general procedure of Example 80 was followed the title compound was obtained. Total yield, 0.38 g (33%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05153226
Source datasetuspto-grants-1992_10
ORD IDord-d1ae2efd19294a3f888d5f51c5dcd1a9
Source noteuspto-grants-1992_10