HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → N-[2-[[2,6-bis(1-Methylethyl)phenyl]amino]-2-oxoethyl]-N-(diphenylmethyl)-2,2,3,3,4,4,4-heptafluorobutanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Heptafluorobutyric anhydride | HCID 67643 | — |
| Reactant | N-[2,6-bis(1-Methylethyl)phenyl]-2-[(diphenylmethyl)amino]acetamide | HCID 1645639 | — |
| Reactant | N-[2,6-bis(1-Methylethyl)phenyl]-2-[(1,1-dimethyl-2-phenylethyl)amino]acetamide | HCID 19874910 | — |
| Product | N-[2-[[2,6-bis(1-Methylethyl)phenyl]amino]-2-oxoethyl]-N-(diphenylmethyl)-2,2,3,3,4,4,4-heptafluorobutanamide | HCID 19874870 | — |
Reaction Steps
When in the procedure of Example 79 an appropriate amount of the product of Example 4 was substituted for the product of Example 5 and an appropriate amount of heptafluorobutyric anhydride was substituted for acetic anhydride and the general procedure of Example 79 was followed the title compound was obtained. Total yield, 1.33 g (59%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05153226 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-dc87ba1364ec41c1901f800b265ed00b |
| Source note | uspto-grants-1992_10 |