HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dimethoxybenzoyl chloride → N-[2-[(2,6-Diethylphenyl)amino]-2-oxoethyl]-N-(diphenylmethyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dimethoxybenzoyl chloride | HCID 87364 | — |
| Reactant | 2-Methoxybenzoyl chloride | HCID 88969 | — |
| Reactant | N-[2,6-bis(1-Methylethyl)phenyl]-2-[(diphenylmethyl)amino]acetamide | HCID 1645639 | — |
| Product | N-[2-[(2,6-Diethylphenyl)amino]-2-oxoethyl]-N-(diphenylmethyl)benzamide | HCID 19874973 | — |
Reaction Steps
When in the procedure of Example 94 an appropriate amount of the product of Example 75 was substituted for the product of Example 4 and an appropriate amount of 2,5-dimethoxybenzoyl chloride was substituted for 2-methoxybenzoyl chloride and the general procedure of Example 94 was followed the title compound was obtained. Total yield, 0.35 g (51%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05153226 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-e1d2905f9dd141739d0344d26637e187 |
| Source note | uspto-grants-1992_10 |