HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isothiocyanic acid, p-dimethylaminophenyl ester → N-(2,6-Diethylphenyl)-2-[[[[4-(dimethylamino)phenyl]amino]thioxomethyl](diphenylmethyl)amino]acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isothiocyanic acid, p-dimethylaminophenyl ester | HCID 75047 | — |
| Reactant | N-[2,6-bis(1-Methylethyl)phenyl]-2-[(diphenylmethyl)amino]acetamide | HCID 1645639 | — |
| Reactant | N-[2,6-bis(1-Methylethyl)phenyl]-2-[(2,2-diphenylethyl)amino]acetamide | HCID 19874997 | — |
| Product | N-(2,6-Diethylphenyl)-2-[[[[4-(dimethylamino)phenyl]amino]thioxomethyl](diphenylmethyl)amino]acetamide | HCID 19874867 | — |
Reaction Steps
When in the procedure of Example 80 an appropriate amount of 4-dimethylaminophenylisothiocyanate was substituted for ethyl isocyanato acetate and an appropriate amount of the product of Example 4 was substituted for the product of Example 70 and the general procedure of Example 80 was followed the title compound was obtained. Total yield, 0.68 g (62%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05153226 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-2c9899b9226d41c5bb67574309d31e3a |
| Source note | uspto-grants-1992_10 |