HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 54338254, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-Methyl-2-butenal | HCID 61020 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 54338254 | HCID 54338254 | — |
Reaction Steps
3-methyl-2-butenal is reacted with chlorotrimethylsilane using the method of P. Cazeau et al., Tetrahedron 43, 2075-2088 (1987), in acetonitrile containing triethylamine and anhydrous sodium iodide at 40°-45° to yield 1-trimethylsilyloxy-3-methyl-1,3-butadiene 2;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05153337 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-b57b5d1801d747d49eb51b93f87f5e25 |
| Source note | uspto-grants-1992_10 |